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Introduction

Research
& Services


 
   RESEARCH & SERVICES

This presentation contains details of the capabilities, activities, research laboratories and technical services expertise which, NNPC Research Development Division can render.

Our activities in the laboratories are covered by the NNPC corporate health and safety policy.

We are in the process of getting the ISO 9000 certification.

We have undoubtedly the best equipped laboratories of its kind in the west Africa sub-region; Our services are cost affective, reliable competitive, and confidential.

CRUDE ASSAY AND PETROCHEMISTRY
 Complete crude oil assay (ASTM, D2892, & ASTM D1160)
 Evaluation of crude oil samples for certain products potential (eg. Lube oil or bitumen production.
 Evaluation of crude oil for:
  (a) Marketing and price determinati6n based on netback policy.
  (b) Products slate changes and refinery production optimisation.
  (c) Design of the refinery
  (d) Refinery equipment performance monitoring.
 Advisory services on crude oil processing.
 Advisory service on petroleum and petrochemical products end-use applications.
 Advisory services on natural gas utilization.

INSTALLED FACILITIES
 H. S. Martins 40L Distillation Unit (LARGE STILL)
 Asphaltene Reactor
 Bench-Top catalyst Tester- (IFP Geomecanique)
 Petroleum products and Crude Oil testing Equipment
 Low Temperature Solvent Distillation Equipments Fischer Minitron)
 Fischer Autodest 851 AC.
 Fischer Autodest 800 AC.

PROCESS AND CATALYSIS
Process and Catalysis is set up to provide complete catalysis development, characterisation, formulation, and synthesis. It also offers process-engineering solutions, corrosion studies and research and material selection for the petroleum industry using engineering software and plants.

A. PROCESS TECHNOLOGY
For complete studies on refinery and petrochemical operations in:
 Process Plant optimization.
 Development of process technologies.
 Monitoring test run for specified objectives.
 Process and energy integration and optimisation of refineries and petrochemicals plants.
 Troubleshooting of refinery and petrochemical plants operations.
 Computer simulation of plant operations.

B. CORROSION STUDIES
Inspection and studies for equipment and pipelines in the following areas:
 Equipment arid pipeline corrosion monitoring.
 Corrosion testing and prevention.
 Systematic evaluation of the impact on material failures on refinery and petrochemical plants operations.
 Studies on anti-corrosion materials and chemicals.
 Prediction, Measurement and Evaluation of Corrosion.

CATALYSIS DEVELOPMENT
 Evaluation of current used catalysts in different processes for performance rating.
 Undertaking research work on:
  (a) Synthesis of Zeolites of known lattice framework structure.
  (b) Synthesis of Zeolites with Novel framework structures.
  (c) Zeolites to enable them to exhibit novel catalytic properties.
  (d) Synthesis of Zeolite with novel Chemical composition and lattice framework structures.
  (c) Establish corrections for Zeolite synthesis.
 Development of selective catalysts.
 Development of industrial scale productions of the novel Zoelite catalysts showing economic viabilities.
 Bench Scale Studies.
 Process optimization

INSTALLED FACILITIES

1. PROCESS ENGINEERING
 HYSYS Engineering solutions software for steady state and dynamic simulation.
 STX Shell and tube exchanger rating, design and evaluation software.
 ACX Air cooled heat exchanger rating, design and evaluation software.
 Other general engineering design software

2. CATALYST EVALUATION RESEARCH
 LAB Micro reactor for static and dynamic auditing evaluation of catalysts performance.
 Low Temperature Fractionation Equipment.
 Bench Top Aromatic Extractor

CATALYSIS DEVELOPMENT
 Scale-up of laboratory set-ups to pilot plant scale.
 Pilot plant studies of refinery and petrochemical processes.
 Reconciliation of pilot plants performance result with that of computer simulation.
 Pilot plant scale-up to commercial unit.
 Simulation and analysis of Refinery and Plants processes using pilot plant.

ENVIRONMENTAL RESEARCH & SERVICES
This Department provides services and expertise to third parties to ensure compliance with government regulations on the environment. We undertake pre and post environmental impact assessments bioremediation studies for the impacted ecosystem by industrial activities.

RESEARCH & SERVICES
 Provides dredging and drilling compliance monitoring services.
 Bioremediation Studies of Impacted Ecosystems.
 Monitoring of Waste Treatment and Solid Waste Disposal Plants.
 Acquisition of Environmental Base-line Data.
 Environmental Impact Assessment Studies for Seismic Exploration Activities, Industrial Development, etc.
 Environmental Sensitivity and Stress Distribution Mapping.
 Consultancy services on pollution problems.
 (Abatement, prevention and control).
 Determination and monitoring of Atmospheric.
 Pollution.
 Toxicity Studies and Tests.
 Environmental Auditing.
 Consultants to the Federal Government of Nigeria.
 FEPA, state Government on environmental issues.

INSTALLED FACILITIES
 Modern Analytical Laboratory supports.
 Ambient Air Monitoring Unit.
 Modem environmental Facilities.

ANALYTICAL RESEARCH AND SERVICES
The Analytical Chemistry Laboratory is a reference Laboratory providing state of the laboratory services such as Spectroscopy, and Elemental Analysis, Chromatography, Water and Special Chemicals analysis, Petroleum Testing and Analysis for the Oil and Gas Industry Operators and Other Bodies in Nigeria.

Reasearch work and services undertaken is as listed below;

SPECTROSCOPY AND ELEMENTAL ANALYSIS
 Metals in water, Wastewater, Organic and Inorganic Materials, Soils, Sediments, Chemicals and other materials.
 Carbon, Hydrogen and Nitrogen, in Organic deposition (Waxes, Hydrates, Asphaltenes).
 Infa-Red (IR), and Ultraviolet (UV-VIS) analysis.
 X-Ray fluorescence Analysis of Geological samples.
 Elemental analysis.
 Crude Oil and Petroleum Products analysis

CHROMATOGRAPHY
GAS CHROMATOGRAPHY
 Natural gas and volatile organic substances analysis.
 Analysis of Petroleum and its products.
 Volatile and non-volatile organic substances from water; soil plants extracts etc.
 Analysis of heavy petroleum distillates.
 Organic materials

WATER AND SPECIAL CHEMICALS ANALYSIS
 Ground and surface water, Wastewater, Sludge
 Sediments, Soil etc.
 Produced Waters
 Oil field and specialty chemicals

PETROLEUM PRODUCTS TESTING/ANALYSIS
 Crude oil
 Petroleum Products including Asphaltic materials
 Lubricants.

INSTALLED FACILITIES
 Gas Chromatograph (GC).
 PIONA Analyser.
 High Performance Liquid Chromatograph HPLC.
 Gas Chromatograph/Mass Spectrometer(GC/MS).
 Atomic Absorption Spectrophotometer(AAS) including:
  (a) Controlled Temperature Furnace
  (b) Hydride Generator
 FT-IR Spectrometer
 CHN Elemental Analyser
 Ion sensing Meter and Electrodes
 Auto -Titractors BOD Apparatus
 PH and Conductivity Meters
 Dissolved Oxygen Meter
 TDS meters
 Energy Dispersive X-ray Fluorescence (EDXRF) Spectrom
 Total Organic Carbon (TOC) Analyser
 Reid Vapour Pressure (RVP) Assembly
 Dean and Stark Apparatus
 Viscosity Assembly
 Aniline Point Apparatus
 ASDM-D-86 Distillation Apparatus
 Flash Point Testers
 Copper Corrosion Testing Assembly
 Potentiograph
 Fluorescence Indicator Absorption assembly (FIA)
 Bomb Calorimeter/Sulphur Analyser Assembly
 X-ray Fluorescence Sulphur Analyser
 Karl-Fischer Apparatus
 Puor Point Tester
 Tensiometer
 Existent Gum Equipment
 KF Coulometer
 Colorimeters
 Asphalt Ductility Tester
 Penetrometer.

EXPLORATION AND PETROLEUM ENGINEERING DEPARTMENT (E&P)
The E&P department provides services and carries out research activities in the upstream sub-sector of the Oil and Gas industry.

It comprises two sections:
1. Exploration Research & Services
2. Petroleum Engineering Research & Services

EXPLORATION RESEARCH AND SERVICES
The Exploration Research and Services section performs geoscientific research and provides consultancy services for basin studies and reservoir modeling. With qualified geoscientists and laboratories equipped with state-of-the-art facilities, it caters for the need of the upstream sector of the oil and gas industry.

GEOPHYSICS
 2D and 3D Data processing Techniques with emphasis on Multiple Suppression and Prospect Characterisation.
 2D and 3D Seismic Data Interpretation.
 Seismic Stratigraphic Evaluation and Interpretation.
 Well Log Interpretation.
 Remote Sensing and Imagery Studies.
 Gravity, Magnetic, Electrical and EM studies and Data Interpretation.
 Integrated Geophysical Studies.
 Geophysical Modelling.

SEDIMENTOLOGY
 Lithostratigraph/Borehole Reservoir, Source and Cap rock identification and characterisation.
 Determination and interpretation of composition, texture, structures and environments of deposition of sediments.
 Thin Section Petrography: Diagenetic studies of sediments (Paragenesis).
 SieveAnalysis.
 Heavy Mineral Analysis.
 Facies Modelling.
 Photogeological Interpretation and Analysis.

BIOSTRATIGRAPHY
 Industrial Palynology; Dinocysts, Acritarchs and Nannolossils Studies.
 Industrial Micropalaeontology: Foraminifera and Ostracode Studies.
 Biostratigraphcal Modelling.
 Correlation Studies.
 Sequence Statigraphy.
 Biozonation.
 Micropalaeontology and Palynological Photography.
 Foraminiferal and Miospore Type Collection.
 Paleogeography.
 Micropaleoontological and Palynological Age determinations.

PETROLEUM GEOCHEMISTRY
 Source Rock Potential Evaluation and Characterisation.
 Thermal maturity Evaluation Using Emperical Methods.
 Total Organic Cabon (TOC) Analysis.
 Vitrinite Reflectance (VR) Analysis Techniques.
 Geochemical Correlation Studies.
 Bitumen Fractionation and Gas chromatographic Studies.
 Pyrolysis studies.
 Kerogen Type determination.
 Clay Mineralogy.

BASIN ANALYSIS
Regional interpretation of the geology of a Petroleum province using the following multidisciplinary geoscientific techniques.
 Well Log Seismic/Sequence Stratigraphy.
 Quantity Stratigraphy.
 Burial and Geohistory Calculations.
 Geochemical Logging.

OTHERS
 Geophysical and Geotechnical site Investigation.
 Soil Investigation.
 Geological Sourcing of Raw Materials.
 Industrial Materials Characterisation.

INSTALLED FACILITIES
 Rock Eval/Oil show Analyser
 Vitrinite Reflectance Microscopes
 Sedimentological Microscopes
 Petrographic Photomicroscopes
 Palynological Photomicroscopes
 Micropalaeontological Photomicroscopes
 Centrifuges
 Rock Cutting Machine for thin Sectioning.
 Palynological Maceration Equipment
 Micropalaentological Processing Materials
 Vibratory sieve Shaker installed with auto sieve system
 Stereoscopes
 Modem Draughting Office
 Analytical Laboratory equipped with GC-Mass Spectrometers, Gas Chromatographs, x-ray Fluorescence, IR, Elemental Analyser. Atomic Absorption Spectrophotometer HRGC, XRD
 Diano X-Rav Diffractometer
 Introscan MK-5 TLC/F ID Analyser
 Scintrex Autograph Automated Gravity meter
 Campu Geopulse Resistance meter.

PETROLEUM ENGINEERING AND SERVICES
Petroleum Engineering Research and Services ranges from the initial appraisal of exploration discoveries through field development, production and reservoir management. Laboratory Programmes are designed to ensure maximum relevant information at minimum cost.

CONVENTIONAL CORE ANALYSIS
 Well site Core Handling/preservation
 Porosity
 Grain Density
 Air Permeability
 Fluid Saturation

SPECIAL CORE ANALYSIS
 Formation Factor
 Saturation Exponent
 Caution Exchange Capacity
 Capillary pressure measurements by mercury injection method
 Capillary pressure measurement by porous plate method

ANCILLARY CORE ANALYSIS
 Sieve Analysis
 Pore Size Distribution Analysis
 Total Core Gamma logging
 Core Photography (ultraviolet and white light)

RESERVOIR ENGINEERING
 Integrated Reservoir Engineering studies
 Detailed Reservoir and Fluid characterisation
 Reservoir Evaluation
 Formation damage studies
 Enhanced oil recovery

PVT ANALYSIS
 Subsurface black/volatile oil sample
 Recombined black/volatile oil sample
 Condensate Reservoir Fluid Sample
 Dry gas sample
 Separator Test at separator Temperature

INSTALLED FACILITIES
 Porosimeter/Gas Permeameter
 Dean-stark Fluid Extraction Equipment
 Soxhlet Fluid Extraction equipment
 Caution Exchange Capacity Equipment
 Restor Equipment
 Conductance-Resistance meter
 Porous Plate capillary pressure apparatus
 Core Slabbing and Plugging equipment
 Mechanical Sieve Analysis equipment
 Autosiever
 Total Core Gamma
 Core Photography equipment for both white & UV lights.

SUPPORT SERVICES

GLASSBLOWING TECHNOLOGY
The NNPC, R&D GLASSBLOWING WORKSHOP carries out design, Fabrication, Calibration, and Screen-Printing as well as repairs to Scientific Glassware to DIN, BS and ASTM standards. Ornamental Glassware are also designed and fabricated to Clients Specifications.

GLASSWARE TYPES
 Adapters, Burettes and Pipettes.
 Dean and Stark Equipment.
 Condenser and Columns.
 Filter Pumps and Flasks.
 Kjedahl Apparatus, Soxhlet Extraction apparatus, etc.
 Measuring Cylinders
 Splash head & Stirrers
 Test Tubes & Thermoflasks
 Wash Bottles.

INSTALLED FACILITIES
 B+C Glass workshop Lathe, Universal model (Swing Type).
 Bell Types Annealing furnace
 Superb Universal Glass/Ceramic cutting machine
 Belt Grinding and Glass Grinding Machine
 Formmaster and Tool Plus Accessories
 Glass boring and Drilling machines
 Universal Glass coil winding machine (B+C Spiralomat)
 Computer controlled Calibrating machine
 Universal screen printing machine
 Flat lapping machine.

REFINING AND PETROCHEMICAL DEPARTMENT(R&P)
The R&D department is set up to carry research and to undertake services in refining and petrochemicals plants and process technology, new products development, environmental science, and analytical Chemistry.

It has four main sections viz:

1. Petroleum Products Research & Services (PPRS).
2. Process and Catalysis (P&C).
3. Environmental Research & Services
4. Analytical services.

KEY AREAS OF RESEARCH AND SERVICES OFFERED
 Development of new products.
 Fuel and Lubes Research.
 Studies on diversification of petroleum product derivatives for end-use application.
 Engine testing.
 Additives formulation.
 Data base on Nigerian export blends and
 Crude oils from different parts of the world

SOLVENTS DEVELOPMENT
 Evaluation of distillates and condensates
 Evaluation of NGLs and condensate as feedstock for solvents products
 Development of paint and ink colours
 Research into new products development
 Research into feedstock for solvent production
 Solvent characterisation
 Feasibility studies for solvent production, from natural Gas, NGLs
 And white distillates

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